Introduction to Shimadzu Atomic Absorption Spectrophotometer AA7000 Instrument

Product Name: AA-7000 Atomic Absorption Spectrophotometer
Product information:
The AA-7000 series atomic absorption spectrophotometer can perform high sensitivity analysis. This model has flexible configuration, compact and exquisite design, and is easy to use. In addition, the AA-7000 system is the world's first AAS standard equipped with vibration sensors. The AA-7000 series ensures efficient and comfortable operation in your laboratory.
World class high sensitivity
The dual beam optical system and stable hardware can achieve extremely high stability.
The AA-7000 series is equipped with a newly developed 3D dual beam optical system, which achieves the best performance of flame and graphite furnace methods through optimization of the beam and beam digital regulator, and reduces light energy loss through optimization of optical components.
World class detection limit
The leading design of the optical system and new graphite furnace significantly improves the detection limit of the graphite furnace (compared to previous Shimadzu models). Excellent performance can play a role in various fields.
Advanced security technology
Safety is an extremely important consideration for the use of acetylene flame atomic absorption spectrometers. The AA-7000 series is the world's first standard equipped with vibration sensors, and is also equipped with comprehensive safety mechanisms, including gas leak detectors.
*Shimadzu Internal Inspection, November 2008
Flexible configuration that changes as needed
The AAC-7000 option can achieve the integration of flame atomizers and graphite furnace atomizers, and make the switching between the two convenient and fast.
*AAC-7000 cannot be installed on AA-7000G.
AA-7000 Basic Specifications
measurement system |
Measure wavelength range |
185~900nm |
monochromator |
Aberrant correction Czerny Turner device |
Number of grating engraved lines |
1800 pieces/mm |
bandwidth |
0.2, 0.7, 1.3, 2.0 nm (4-speed automatic switching) |
detector |
Photomultiplier tube |
Photometric measurement method |
Flame: Optical Dual Beam
Graphite furnace: electronic dual beam
|
Background correction |
High speed self absorption (BGC-SR), with a self absorption frequency of not less than 100Hz
High speed deuterium lamp method (BGC-D2), with a deuterium lamp frequency of not less than 1000Hz. Hollow cathode lamp frequency not less than 500Hz
|
Number of lamp sockets |
6 lamp sockets, 2 lamps light up simultaneously (1 preheating) |
lighting system |
Launch, NON-BGC,BGC-SR,BGC- D2 |
Baseline stability |
0.004Abs/30min |
data processing |
software environment |
Microsoft Windows 2000/xpTM |
Parameter settings |
Wizard method |
Measurement method |
Flame continuous method, flame micro injection method, graphite furnace method |
Concentration conversion method
|
Calibration curve (can choose 1st, 2nd, 3rd order function)
Standard addition method/simplified standard addition method (first-order function)
|
repeated measurement |
Up to 20 repetitions
Display mean, standard deviation (SD), and relative standard deviation (RSD)
Automatically exclude outliers based on standard deviation (SD) and relative standard deviation (RSD) values
|
baseline correction |
Using peak height and peak area offset correction method to automatically correct baseline drift |
Peak data processing range |
Peak data processing range, with optional peak height and peak area methods. |
Sensitivity correction |
Automatically calibrate the calibration curve through sensitivity comparison |
Analog Output |
Dual channel (atomic absorption/energy signal and background signal)
Output range: 5.0, 2.5, 1.25, 0.625Abs/V (with four gear switches each)
EMISSION is fixed at 1VF S.
|
Table data processing function |
Calculate the actual sample concentration using weight factor, dilution factor, constant volume factor, and correction factor. |
Loading parameters |
Template function available |
multitasking |
During the measurement process, other software such as MS Office can be used |
Step/result display |
MRT Work Order (MRT: Measurement Results Table) |
Result printing |
Summary report |
QA/QC |
Correlation coefficient,% After RSD, ICV/ICB, CCV/CCB, PB, LCS, SPK, PDS, DUP, QA/QC inspections, analysis can be paused, marked, or resumed |
Retesting |
You can choose whether to retest.
Automatic sampler automatically dilutes unknown samples and re measures them (flame microinjection method, graphite furnace method)
|
Electronic Records and Electronic Signatures |
Registration ID/Password User Management
Permissions granted by user level restrictions
Log recording
Track and review
Electronic Signature
|
Requirements for power supply |
AC220V, 230VA, 50/60Hz, with additional power for PC. |
Size and weight |
AA-7000F: Length 700 x Width 588 x Height 714 mm, 72 kg
AA-7000G: Length 700 x Width 580 x Height 538 mm, 65 kg
(Excluding protruding parts and optional items)
|
Range of environmental temperature and humidity
|
10°C~35°C,20%~80%
If the temperature exceeds 30 ° C, the humidity should be less than 70%
|
Flame specifications
Burner unit |
type |
Air-cooled premixed type |
Burner head |
10cm titanium (5cm titanium, used for N2O-C2H2 flame, optional) |
atomizer |
Pt Ir capillary tube, PTFE nozzle, ceramic impact ball (can be used for hydrofluoric acid) |
Atomization chamber |
Specially treated polypropylene |
Position adjustment
|
AA-7000F:
Manually adjust the front, back, up, and down positions
AA-7000F (when installing the atomizer automatic switching device):
Automatic adjustment of front, back, up, and down positions
Automatically search for the optimal burner height
|
|
Angle adjustment |
0-90 degrees |
Gas controller |
flow control |
Automatic setting of gas and auxiliary gas flow rate (0.1 L/min increment)
Automatic setting of auxiliary gas flow rate (when installing optional components)
Automatically search for the optimal gas flow rate
|
safety performance |
Automatic leak detection
Automatically switch the flow rate of air/N2O according to C2H2
flame monitor
Prevent misuse of burner heads
Gas pressure monitor
Waste liquid level monitor
Automatic detection of instantaneous power outage and safe shutdown function
Using vibration sensors to safely shut down the engine
Stop detection of fan inside the instrument
|
sensitivity |
The absorbance of 2ppm Cu is about 0.32Abs
Detection limit of Cu: not greater than 0.004Pm
|
Graphite furnace specifications
Heating temperature range |
Room temperature~3000 ° C |
Heating control method |
Drying: Current control method (with automatic temperature correction function) |
Ashing/Atomization: Optical Temperature Control Method |
Heating parameter setting |
Maximum heating rate: 3000 ° C/second |
Up to 20 segments |
Heating method: slope/step |
Internal gas type: 2-way switching |
High sensitivity setting |
Graphite furnace concentration enrichment cycle: up to 20 cycles |
Optimal graphite furnace program search function |
Internal gas flow rate: 0-1.5 L/min, gas control accuracy can reach 0.01L/min |
sensitivity |
Detection limit of Pb: 0.05ppb |
safety performance |
Cooling water flow monitor |
Gas pressure monitor |
Overcurrent protection (dual monitoring of circuit breaker and optical probe) |
Inspection of graphite furnace cooling block |
Position adjustment of graphite furnace |
AA-7000G
Front back/up and down manual adjustment
AA-7000F (Installation of Atomizer Automatic Switching Device)
Automatic switching of motor drive for combustion head/graphite furnace
Automatic adjustment of front, back, up, and down positions
|
autosampler
One machine dual-use, capable of meeting the needs of both flame and graphite furnace simultaneously
One automatic sampler host can be used for both flame analysis and graphite furnace analysis, with universal specifications for flames and graphite furnaces
Function: Origin detection function; Automatic cleaning function; Self diagnostic function; Random arrangement
Maximum number of samples: 8 samples for reagents and 60 samples (all can be randomly arranged)
Sample container: 15ml (flame specific test tube) or 2ml (graphite furnace specific sample vial)
53ml reagent container (flame specific test tube) or 20ml reagent container (graphite furnace specific test tube)
Spray nozzle cleaning: solvent discharge method (during graphite furnace measurement) solvent suction method (during flame measurement)
Cleaning solution bottle: 2L
Special specifications for graphite furnace
Sampling function: dilution function, reagent addition function
Syringe: 250 μ l
Injection volume: 2-90 μ l
Reproducibility: 1% R.S.D (at 20 μ l)
Cross contamination: cleaning port below 0.00001, mixing port below 0.00001
Mixing port cleaning: solvent discharge method, sample co washing method
Mixing function: using a mixing port, the maximum capacity that can be mixed is 600 μ l
Number of reagents added: up to 4 liquids, the injection sequence of samples and reagents can be set (when not mixed)
Number of Mixable Liquids: Working Curve Method: Up to 5 Liquids Standard Addition Method: Up to 6 Liquids
Automatic dilution and retesting: judge the results of unknown samples based on the working curve. When using the extension method, the dilution factor is automatically calculated based on the range of the working curve for dilution. When the extension method is not possible, the dilution factor should always be 10 times