Integrated intelligent distiller price, ammonia nitrogen automated distillation device manufacturer price

This product adopts intelligent integrated equipment, using PTC (far infrared ceramic heating) technology instead of high-power electric heaters, and adopts intelligent distillation endpoint control. The built-in cooling water self cooling and piano playing system, as well as special customized condenser tubes and other technical means, achieve the goals of simple operation, automatic distillation, beauty and practicality, energy saving and consumption reduction. It can be widely used in environmental monitoring, water supply and drainage, hydrological monitoring, product quality inspection, inspection and quarantine, scientific research institutes, universities, disease prevention and control centers and other chemical laboratories that require distillation treatment. It is suitable for the volatile phenols, ammonia nitrogen, water content in oil, residual sulfur dioxide in food testing, formaldehyde (suspended white blocks), alcohol content, chemical oxygen demand of high chlorine wastewater, calibration method distillation operation, etc.

1： Technological innovation points

1. This product is a laboratory distillation device with an integrated design of heating, distillation, cooling, and receiving, and is one of the essential instruments for distillation projects at all levels of laboratories

2. Adopting far-infrared ceramic heating technology, infrared radiation heating (no open flame heating, waterproof). The power consumption is only one fourth of the original high-power electric heating, but the effect is equivalent to that of ceramic heaters being water-resistant, avoiding water flooding and causing circuit short circuits

3. Adopting a built-in cooling water circulation system and automatic cooling technology, there is no need for external tap water cooling, saving a lot of rich and prosperous urban freshwater resources

The distillation endpoint adopts an infrared sensing device. When the distillate reaches the distillation endpoint, the infrared liquid level sensing automatically starts and stops heating, which can achieve unmanned operation of the distillation process

5 instruments can produce 6 sets of samples at a time, with 6 holes that can be individually controlled. The heating temperature and heating time are automatically displayed on the large LCD screen

The end of the distillate is equipped with an anti backflow device and a vacuum electromagnetic valve to ensure one-way flow of the distillate and prevent backflow back into the flask

The snake shaped condenser tube designed with 7 technologies has fast distillation speed and good cooling effect

Ammonia nitrogen distiller

2： Technical parameters of intelligent integrated distillation apparatus for water quality monitoring

1. Heating method: using imported far-infrared ceramic heating furnace, infrared radiation heating (no open flame heating, waterproof);

2. Heating units: 6, single hole single control;

3. Heating time: 5-8 minutes;

4. Distillation speed: 12ml/min;

5. Distillation endpoint control: automatic detection of distillation endpoint function, using dual control of weighing and time, with distillation volume controlled within ± 2ml, high degree of automation;

6. Single furnace heating power: 0-450W (single hole adjustable);

7. Heating power: 0-2700W (adjustable);

8. Cooling method: Closed internal circulation reflux system, no need for external cooling water source;

9. Anti reverse suction: equipped with anti vacuum solenoid valve, with anti reverse suction function;

10. Time control: adjustable from 0-200 minutes;

11. Distillation flask specifications: 500ml X6250 X6. More specifications are available;

12. Rated voltage/frequency: 220V/50HZ;

Model Speed Heating Power Function

BY-ZL6B Distillation speed: 12ml/min Heating power: 0-2700W Ordinary type: Heating+timing, air-cooled

BY-ZL6D Distillation speed: 12ml/min Heating power: 0-2700W Intelligent type: Heating+Timing+Weighing, Water cooling

1. Add the distilled sample, required reagents, zeolite, water, etc. into the distillation flask in sequence and mix well.

Place the flasks in the heating holes one by one and seal them with the condenser tube.

Connect the outlet of the condenser tube distillation solution to the receiving bottle.

4. Place the receiving bottle tightly against the distillation endpoint probe, and adjust the position of the distillation endpoint probe if necessary (the position of the distillation endpoint probe has been adjusted before leaving the factory, if adjustment is needed, please contact the manufacturer)

Turn on the power switch and design the required heating temperature and working time (default settings from the instrument factory)

6. Turn on the circulating cold water switch to allow the cooling water to circulate automatically

Press the switch for heating holes 1-6 as needed, and press the start button to start working.

When the distillate reaches the required liquid level, the instrument will automatically stop heating and shut down after distillation is completed.

4： Precautions

When the temperature in summer exceeds 25 degrees, the cooling effect will decrease. It is recommended to use an external cooling water circulation device (BA-ZL6D) or an external tap water cooling device (BA-ZL6A) for cooling

When the room temperature is below 0 degrees Celsius in winter, it is necessary to do a good job of keeping the instrument warm to prevent condensation devices from bursting and causing it to be unusable.

When adding cooling water for the first time, it is recommended to use pure water or distilled water to prevent the formation of scale after long-term use. A full tank can circulate for more than six months

During the heating process, for instruments or sewage samples with severe boiling phenomenon, the heating power knob can be adjusted to gradually increase the heating power, or a few pieces of glass or organic silicon anti foaming agent can be added appropriately.

Integrated intelligent distiller price, ammonia nitrogen automated distillation device manufacturer price

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The condenser bottle 5 includes a bottle body 51 and a spiral condenser tube 52 inside the bottle body 51. The upper end of the bottle body 51 is provided with a steam inlet 56, the lower end is provided with a distilled liquid outlet 55, and the side is provided with a cooling water inlet 54 and a cooling water outlet 55. Both the cooling water inlet 54 and the cooling water outlet 55 are connected to the cooling water device 13. Through the built-in circulating cooling water device, the distillation equipment is integrated, reducing the amount of equipment used during distillation.

Working principle: When conducting distillation, the distillation bottle 3, reflux bottle 2, safety bottle 4, condensing bottle 4, and cooling water device 13 of this utility model can be used separately as a set of distillation equipment, or multiple distillation bottles 3 can be distilled simultaneously. The heating temperature of each electric heating jacket 12 is controlled by the heating control switch 15 to heat the distillation bottles 3. When multiple distillation bottles 3 are distilled simultaneously, the cooling water device 13 is connected to the cooling water inlet 54 of the first condensing bottle, and then the cooling water outlet 55 of the first condensing bottle is connected to the cooling water inlet 54 of the next condensing bottle, and so on, until the cooling water outlet 55 of the last condensing bottle is connected back to the cooling water device 13. After multiple uses, the cooling water refluxes. Inside the cooling water device 13, water resources are saved and the number of distillation instruments is reduced, Detect the water level inside the cooling water device at any time through the liquid level observation window 10, and add it in a timely manner when it is insufficient.

The above embodiments are only the preferred embodiments of the present utility model and do not limit the technical solution of the present utility model. Any technical solution that can be implemented on the basis of the above embodiments without creative labor should be considered to fall within the scope of protection of the present utility model patent.

On the other hand, the heating of the blowtorch requires manual heating, which makes it difficult to accurately control the heating temperature, resulting in significant errors in the analysis data and poor repeatability.

[0007]

[Invention Content]

[0008] The purpose of the present invention is to provide a novel distillation apparatus with simple structure, high efficiency, accurate data analysis, good repeatability, and convenient operation.

[0009] To solve the above technical problems, the present invention provides a novel distillation apparatus comprising a frame, a distillation flask, a condenser tube, and a reflux flask. The frame is provided with a heating bath and a heating chamber, the condenser tube passes through the heating bath, the reflux flask is provided in the heating chamber, the distillation outlet of the condenser tube is provided in the heating chamber, the frame is provided with a kitchen door on the outside of the heating chamber, and the heating bath is a water bath or an oil bath.

[0010] In order to reduce the deformation of the kitchen door due to high temperature, the present invention is improved by using fiberglass as the material of the kitchen door.

[0011] In order to maintain the liquid state of the distillate, the present invention is improved by providing a heater in the heating chamber.

[0012] For the convenience of temperature control, the present invention is improved by installing a cooling fan inside the heating chamber.

[0013] The improvement of the present invention is that the heater is an electromagnetic heater, an infrared heater, or a resistance heater.

[0014] In order to achieve accurate temperature regulation, the present invention is improved by installing a temperature sensor inside the heating chamber.

[0015] In order to improve data repeatability, the present invention is improved by providing a stirrer inside the heating bath.

[0016] The present invention is improved by using cottonseed oil, glycerol, paraffin oil, cylinder oil, or phenyl silicone oil as the heating carrier for the oil bath.

[0017] The beneficial effects of the present invention are as follows: the distillation apparatus with a new structure, due to the improved overall controllability of the equipment, reduces the analysis time of a single sample by 50% and improves work efficiency by 100%. The old instrument can analyze one sample in 40 minutes per person. The new instrument can analyze four samples in 40 minutes per person, avoiding the use of liquefied gas, reducing safety hazards and energy consumption. In addition, the operation of the entire machine is very simple and easy for employees to learn.

[0018]

[Patent Illustrations]

[Attached Figure Explanation]

[0019] Figure 1 is a schematic diagram of the structure of the new distillation apparatus of the present invention.

[0020] Label Description: 1-Rack; 2. Steam feeding bottle; 3_ Heating bath; 4_ Heating chamber; 5_ Kitchen door; 6-Heater; 7-Cooling fan; 8-Temperature sensor; 9-Blender.

[0021]

[Specific Implementation Method]

[0022] In order to provide a detailed explanation of the technical content, structural features, achieved objectives, and effects of the present invention, the following will be described in conjunction with the embodiments and accompanying drawings.

[0023] Please refer to Figure 1. The present invention provides a novel distillation apparatus, comprising a frame 1, a distillation flask 2, a condenser tube, and a reflux flask. The frame 1 is equipped with a heating bath 3 and a heating chamber 4. The condenser tube passes through the heating bath 3, and the reflux flask is set in the heating chamber 4. The outlet of the condenser tube is set in the heating chamber 4. The frame 1 is equipped with a kitchen door 5 on the outside of the heating chamber 4. The heating bath 3 is a water bath or an oil bath.

[0024] The new structure of the distillation apparatus does not have specific restrictions on the heating of distillation bottle 2, and traditional heating methods can be used. After heating, the gas flows into the condenser tube, which is heated by a water bath (adjusted to a thermal oil bath depending on the situation). The temperature of the water bath heating can reach 95 ° C, and the temperature of the thermal oil bath can reach 150 ° C.

[0025] - In general, the condenser tube can be heated directly using a water bath, using water with the highest specific heat capacity as the heating medium, which saves valuable time for sample cleaning in case of unexpected equipment interruption. Of course, this effect can also be achieved when using a thermal oil bath.

[0026] By using oil bath heating instead of the previous hydraulic gas open flame heating method, the safety factor is greatly improved, and the probability of combustion and explosion caused by condensation is reduced to zero.

[0027] In this embodiment, the heating carrier of the oil bath is specifically cottonseed oil, glycerin, paraffin oil, cylinder oil, or phenyl silicone oil, which can effectively uniformly heat the condensing part.

[0028] In this embodiment, the material of the kitchen door 5 is fiberglass, which is different from traditional plastic materials, reducing the need for cabinet door replacement due to high temperature deformation (reducing consumables), and facilitating cleaning.

[0029] In this embodiment, a heater 6 is installed inside the heating chamber 4, which can effectively control the temperature inside the heating chamber 4, so that the distillate can remain liquid and read volume data in a timely manner. Specifically, the heater 6 can be an electromagnetic heater, an infrared heater, or a resistance heater. It is preferred to use a resistance heater, which can be a resistance wire heater, a ceramic heater, a resistance coil heater, or a quartz tube heater, etc., effectively reducing the temperature gradient of the condensation part, increasing the liquefaction rate of the distillate to 100%, reducing the residual liquid amount and retention time of the condensation part, improving data accuracy, and reducing equipment operation time.

[0030] In this embodiment, a cooling fan 7 is installed inside the heating chamber 4. By setting the cooling fan 7, the temperature of the entire heating chamber 4 can be effectively adjusted to adapt to different conditions of anthracene oil distillation.

[0031] Furthermore, a temperature sensor 8 is installed in the heating chamber 4, which senses the temperature of the distillation outlet and feeds it back to the controller of the entire distillation apparatus. The controller adjusts the operation of the heater 6 and the cooling fan 7 to regulate the temperature of the entire heating chamber 4. The controller can use PLC or microcontroller. The heating bath 3 is equipped with a stirrer 9, which stirs the entire water bath or oil bath to evenly mix the air and heating bath 3, ensuring accurate temperature and good data repeatability.

[0032] The distillation apparatus with a new structure has reduced the analysis time of a single sample by 50% and increased work efficiency by 100% due to the improved overall controllability of the equipment. The old instrument can analyze one sample in 40 minutes per person. The new instrument can analyze four samples in 40 minutes per person, avoiding the use of liquefied gas, reducing safety hazards and energy consumption. In addition, the operation of the entire machine is very simple and easy for employees to learn.