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High purity oxygen analysis helium ion chromatograph
The GC-9560-HG high-purity oxygen analysis helium ion chromatograph is suitable for detecting trace impurities in high-purity oxygen, with a detection
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GC-9560-HGHigh purity oxygen analysis helium ion chromatographSuitable for high-purity oxygenH2Ar、N2、 CH4、 CO、CO2Common impurities or C1-C4Waiting for hydrocarbonsFor the detection of trace impurities in gases, the instrument is equipped with a high-sensitivity helium ionization (PDIHID) detector, using center cutting and blowback technology, equipped with an injection switching valve with a blowback protection gas path and an imported helium purifier. Through non dead volume sampling or online injection methods, H in high-purity oxygen can be completed in one go2Ar、N2、 CH4、 CO、CO2Common impurities and C1-C4The detection limit for hydrocarbons reaches ppb level, with a repeatability RSD of ≤ 1%.
The national standard GB/T 28726-2012 "Gas Analysis - Helium Ionization Gas Chromatography Method", which was mainly drafted by Hua Ai Chromatography, has been officially announced and implemented since February 1, 2013.

1、 Applicable standards:

  • GB/T 14599-2008 "Pure Oxygen, High Purity Oxygen, and Ultra Pure Oxygen"
  • GB/T 28125.1-2011 "Determination of Hazardous Substances in Air Separation Processes"
  • GB/T 28726-2012 "Gas Analysis - Helium Ionization Gas Chromatography Method"

IIHigh purity oxygen analysis helium ion chromatographTechnical parameters:

1. Detection limit (ppb):

General impurities

Types of groceries

H2

N2

CH4

CO

CO2

inspectmeasurelimit

5

10

5

25

5

hydrocarbon

Types of impurities

C2H4

C2H6

C3H6

C3H8

C4H8

C4H10

iC4H10

inspectmeasurelimit

20

20

20

20

20

20

20

2. Temperature control indicators:

  • Column box: 8 ℃ -400 ℃ at room temperature with an accuracy of ± 0.1 ℃
  • Sample injector: Accuracy ± 0.1 ℃ at room temperature between 8 ℃ and 400 ℃
  • Detector: Accuracy ± 0.1 ℃ at room temperature between 8 ℃ and 400 ℃
  • Temperature control quantity: eight channels
  • Program heating: 8th order
  • Heating rate: 1 ℃~40 ℃
  • Cooling rate: within 7 minutes (350 ℃ to 50 ℃)

3. Helium ionization detector (PDD):

  • Discharge mode: Pulse discharge
  • Baseline noise: ≤ 0.1mv
  • Baseline drift: ≤ 0.5mv/30min
  • Detection limit: ≤ 1.0 × 10-10g/ml

4. Carrier gas purifier:

  • Purified gases: He, Ar, Ne, Kr, Xe, Rn
  • Maximum operating pressure: 1000Psi
  • Gas removal: H2、 O2, N2, CO, CO2, CH4, H2O, NO, NH3, CF4, etc
  • Residual concentration: ≤ 10pppb

5. Workstation performance:

  • Communication interface: RS232/USB interface
  • High precision: 24 bit high-precision A/D
  • Resolution: ± 1UV
  • Input voltage range: -5mv to+1v
  • Sampling frequency: maximum 20 times/second
  • Dynamic range: 106
  • Integral sensitivity: 1 μ v • sec
  • Linearity:<± 0.1%.
  • Reproducibility: 0.06%.

6. Other parameters: size, weight, power supply:

  • Dimensions: Width 655mm x Height 500mm x Depth 480mm
  • Weight:~48kg
  • Power supply: 220V ± 22V, 50Hz, power ≥ 2kW

3、 System configuration:

(1) GC-9560-HG high-purity oxygen analysis helium ion chromatograph (2) helium ionization detector (PDIHID)
(3) Central cutting system (4) multi column box system
(5) Helium Purifier (6) Standard Gas
(7) Chromatography Column (9) Oxygen Adsorption and Reduction System
(10) Special pressure reducing valve for carrier gas (11), no dead volume dedicated sampling valve
(12) GC-9560V4.0 Reverse Chromatography Workstation

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